3.4.4 Apparatus 201

3.4.5 Sample Pretreatment 201

3.4.6 Determination 203

3.4.7 Precision 204

Researchers 204

3.5 Determination of 497 Pesticides and Related Chemical

Residues in Honey, Fruit Juice, and Wine: GC-MS Method(GB/T 19426-2006) 204

3.5.1 Scope 204

3.5.2 Principle 204

3.5.3 Reagents and Materials 213

3.5.4 Apparatus 214

3.5.5 Sample Pretreatment 214

3.5.6 Determination 215

3.5.7 Precision 216

Researchers 217

3.6 Determination of 486 Pesticides and Related Chemical

Residues in Honey: LC-MS-MS Method (GB/T 20771-2008) 217

3.6.1 Scope 217

3.6.2 Principle 217

3.6.3 Reagents and Materials 217

3.6.4 Apparatus 227

3.6.5 Sample Pretreatment 227

3.6.6 Determination 228

3.6.7 Precision 232

Researchers 232

3.7 Determination of 478 Pesticides and Related Chemical

Residues in Animal Muscles: GC-MS Method(GB/T 19650-2006) 232

3.7.1 Scope 232

3.7.2 Principle 232

3.7.3 Reagents and Materials 232

3.7.4 Apparatus 242

3.7.5 Sample Pretreatment 242

3.7.6 Determination 243

3.7.7 Precision 244

Researchers 244

3.8 Determination of 461 Pesticides and Related Chemical

Residues in Animal Muscles: LC-MS-MS Method(GB/T 20772-2008) 245

3.8.1 Scope 245

3.8.2 Principle 253

3.8.3 Reagents and Materials 253

3.8.4 Apparatus 254

3.8.5 Sample Pretreatment 254

3.8.6 Determination 256

3.8.7 Precision 257

Researchers 257



4. Determination of 450 Pesticides and Related

Chemical Residues in Drinking Water: LC-MS-MS Method (GB/T 23214-2008) 259

4.1 Scope 259

4.2 Principle 259

4.3 Reagents and Materials 259

4.4 Apparatus 268

4.5 Sample Pretreatment 269

4.5.1 Preparation of Test Sample 269

4.5.2 Extraction 269

4.5.3 Clean-up 269

4.6 Determination 269

4.6.1 LC-MS-MS Operating Condition 269

4.6.2 Qualitative Determination 271

4.6.3 Quantitative Determination 271

4.7 Precision 272

Researchers 272



5. Basic Research on Chromatography-Mass Spectroscopy

Characteristic Parameters of Pesticide and Chemical Pollutants 273

5.1 Mass Spectrometry Data of 1200 Pesticides and Chemical

Pollutants Determined by GC-MS, GC-MS-MS, and LC-MS-MS 277

5.1.1 Retention Times, Quantifier and Qualifier Ions of

567 Pesticides and Chemical Pollutants Determined by GC-MS 277

5.1.2 Monitoring of Selected Ions for 567 Pesticides

and Chemical Pollutants Determined by GC-MS 311

5.1.3 Retention Time, Quantifier and Qualifier Ions, and

Collision Energies of 454 Pesticides and Chemical Pollutants Determined by GC-MS-MS 321

5.1.4 Monitoring of Selected Ions for 454 Pesticides

and Chemical Pollutants Determined by GC-MS-MS 349

5.1.5 Retention Time, Quantifier and Qualifier Ions,

and Collision Energies of 284 Environmental Pollutants by GC-MS-MS 356

5.1.6 Retention Times, Selective Ions, and Relative Abundances

of Endosulfans Determined by GC-NCI-MS 374

5.1.7 Retention Times, Quantifying and Qualifying Ions,

Declustering Potentials, and Collision Energies of 9 Environmental Pollutants Determined by LC-MS-MS 375

5.1.8 Retention Times, Quantifying and Qualifying Ions,Fragmentor, and Collision Energies of 569 Pesticides

and Chemical Pollutants Determined by LC-MS-MS 376

5.1.9 Accurate Masses, Retention Times, Parent Ions,and Collision Energies of 492 Pesticides and Chemical

Pollutants Determined by LC-TOF-MS 410

5.2 Linear Equation Parameters of 1200 Pesticides and

Chemical Pollutants Determined by GC-MS, GC-MS-MS,and LC-MS-MS 457

5.2.1 Linear Equations, Linear Ranges, and Correlation

Coefficients of 567 Pesticides and Chemical Pollutants Determined by GC-MS 457

5.2.2 Linear Equations, Linear Ranges, and Correlation

Coefficients of 466 Pesticides and Chemical Pollutants Determined by GC-MS-MS 491

5.2.3 Linear Equations, Linear Ranges, and Correlation

Coefficients of 284 Environmental Pollutants Determined by GC-MS-MS 519

5.2.4 Linear Equations, Linear Ranges, and Correlation

Coefficients of Endosulfans Determined by GC-MS(NCI) 536

5.2.5 Linear Equations, Linear Ranges, and Correlation

Coefficients of 9 Environmental Pollutants Determined by LC-MS-MS 537

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农业/林业 农业基础科学

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