9.7.3 Reagents and Materials 358

9.7.4 Apparatus 359

9.7.5 Sample Pretreatment 360

9.7.6 Determination 361

9.7.7 Precision 362

9.7.8 Recovery 362

Researchers 363



10. Glucocorticoid 365

10.1 Determination of Nine Glucocorticoid Residues in Fugu, Eel, and Baked Eel—LC-MS-MS Method

(GB/T 22957-2008) 365

10.1.1 Scope 365

10.1.2 Principle 365

10.1.3 Reagents and Materials 365

10.1.4 Apparatus 366

10.1.5 Sample Pretreatment 367

10.1.6 Determination 367

10.1.7 Precision 369

10.1.8 Recovery 371

Researchers 371



11. Fluoroquinolone 375

11.1 Curative Effects and Side Effects of Quinolones 375

11.2 Pharmacokinetics of Quinolones 376

11.3 Chemical Structures and Maximum Residue Limits for Quinolones 376

11.4 Determination of 15 Quinolone Residues in Eel and Eel Products—LC-MS-MS Method 376

11.4.1 Scope 376

11.4.2 Principle 380

11.4.3 Reagents and Materials 380

11.4.4 Apparatus 380

11.4.5 Sample Pretreatment 380

11.4.6 Determination 381

11.4.7 Precision 384

11.4.8 Recovery 385

Researchers 385

References 391

11.5 Determination of Enrofloxacin, Danofloxacin,Ciprofloxacin, Sarafloxacin, Orbifloxacin, Difloxacin, and

Marbofloxacin in Milk and Milk Powder—LC-MS-MS Method (GB/T 22985-2008) 391

11.5.1 Scope 391

11.5.2 Principle 392

11.5.3 Reagents and Materials 392

11.5.4 Apparatus 393

11.5.5 Sample Pretreatment 393

11.5.6 Determination 394

11.5.7 Precision 395

11.5.8 Recovery 399

Researchers 400

11.6 Method for the Determination of 14 Quinolone

Residues in Honey—LC-MS-MS Method (GB/T 20757-2006) 401

11.6.1 Scope 401

11.6.2 Principle 401

11.6.3 Reagents and Materials 401

11.6.4 Apparatus 402

11.6.5 Sample Pretreatment 402

11.6.6 Determination 403

11.6.7 Precision 404

11.6.8 Recovery 406

Researchers 410



12. Tetracyclines 411

12.1 Curative Effect and Side Effects 411

12.2 Chemical Structures and Maximum Residue Limits for Tetracyclines 411

12.3 Determination of Oxytetracycline, Tetracycline,Chlortetracycline, and Doxycycline Residues in

Edible Animal Muscles—LC-UV Method (GB/T 20764-2006) 413

12.3.1 Scope 413

12.3.2 Principle 413

12.3.3 Reagents and Materials 413

12.3.4 Apparatus 414

12.3.5 Sample Pretreatment 414

12.3.6 Determination 415

12.3.7 Precision 415

12.3.8 Recovery 417

Researchers 418

Further Reading 418

12.4 Determination of Oxytetracycline, Tetracycline,Chlortetracycline, and Doxycycline Residues in Milk

and Milk Powder—HPLC-UV Method (GB/T 22990-2008) 418

12.4.1 Scope 418

12.4.2 Principle 418

12.4.3 Reagents and Materials 419

12.4.4 Apparatus 419

12.4.5 Sample Pretreatment 420

12.4.6 Determination 420

12.4.7 Precision 421

12.4.8 Recovery 423

Researchers 424

12.5 Determination of Oxytetracycline, Tetracycline,Chlortetracycline, and Doxycycline Residues in

Fugu and Eel—HPLC-UV Method (GB/T 22961-2008) 424

12.5.1 Scope 424

12.5.2 Principle 424

12.5.3 Reagents and Materials 424

12.5.4 Apparatus 425

12.5.5 Sample pretreatment 426

12.5.6 Determination 427

12.5.7 Precision 427

12.5.8 Recovery 429








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农药兽药多组分残留质谱分析技术:第2卷:Volume Ⅱ:兽药:Veterinary drugs 作者简介

庞国芳，中国检验检疫科学研究院，研究员，中国工程院院士，国家质检总局首席研究员、国际公职化学家联合会（AOAC）专家，国际AOAC 2014年度 Harvey W. Wiley 奖获得者。近30年一直工作在食品检验检疫一线，致力于食品科学检测技术理论与实践的研究，解决了我国相关出口食品、农产品等遭遇的技术瓶颈，为推动我国对外贸易发展做出了杰出贡献。研究制定了141项国际、国家检测技术标准。在国内、国际出版食品安全检测技术论著10部。发表论文100余篇，35篇被SCI收录。3次荣获国家科学技术进步二等奖，6次荣获国际AOAC组织颁发的科学技术奖励。

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